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991.
用粉末冶金真空烧结法制备了超细晶粒碳氮化钛[Ti(C,N)]基金属陶瓷.研究了原始粉末粒径对Ti(C,N)基金属陶瓷微观结构和力学性能的影响.结果表明:在化学成分相同的条件下,晶粒细化使材料的Vickers硬度和抗弯强度上升,但断裂韧性有所下降.在超细晶粒Ti(C,N)基金属陶瓷微观组织中出现了一种新型的白芯/灰壳结构和一种特殊化合物(Ni2Mo2.5W1.3)Cx.初步研究表明:由于原始粉末粒径微小,促进了扩散反应因而生成了这种芯/壳结构.芯/壳结构有利于提高材料的抗弯强度和断裂韧性.(Ni2Mo2.5W1.3)Cx有利于提高材料的Vickers硬度,但是降低了Ti(C,N)基金属陶瓷的抗弯强度和断裂韧性. 相似文献
992.
993.
994.
联合收获机的作业参数与作业性能密切相关,为了满足联合收获机作业性能的实时监测需求,设计了谷物状态监测装置采样盒及其减振器。采用动力学原理分析了联合收获机作业过程中阻流阀往复运动的“采样-卸样”动作特性;运用能量守恒原理建立了有约束条件的减振器保守系统动力学模型;利用多体动力学分析软件ADAMS建立了减振器动力学模型的虚拟样机并进行了求解,通过田间试验验证了该装置的可行性。对比无减振器作业情况,有减振器时谷物状态监测装置获取的图像中籽粒和杂质边缘清晰,图像质量更高;在同样的图像处理算法下,有减振器时破碎率监测结果精度提升了13.7%,监测精度达到了81.3%,含杂率监测结果精度提升了33.6%,精度达到了86.0%。 相似文献
995.
Epifluorescence microscopy study of a quadruple node of triple junctions of grain boundaries in a Eu2+‐doped Kcl:Kbr solid solution by using the doping ion as a fluorochrome 下载免费PDF全文
A typical quadruple node (QN) of triple junctions (TJs) of grain boundaries (GBs) in a Eu2+‐doped KCl0.52Br0.48 solid solution is investigated from the geometrical point of view by epifluorescence microscopy using the doping ion as a fluorochrome. The excitation and fluorescence optical properties of the fluorochrome were previously characterised by spectrophotometry whereas the structural nature of the studied material as well as its Bravais lattice type, unit cell size and long‐range translational order degree was determined by X‐ray diffraction. A three‐dimensional reconstruction was built from the microscopy images of different optical cross‐sections of the studied arrangement of crystal defects. In the close vicinity of the QN, the studied arrangement of crystal defects adopts the geometry of a collapsed tristetrahedron which, centred at the QN, has its legs along the TJs and, hence, has its faces as collapsed in pairs into the GBs. The angles defined by different TJ couples as well as the dihedral angles defined by the different GB couples meeting in every TJ were measured at the QN site. All, the image recording and stacking as well as the measuring procedures are carefully described. The measured TJ angles (97°, 117°, 95°, 117°, 99° and 130° ± 2°) depart from the characteristic angle (109.47°) of a tetrahedron whereas the measured GB angles (101°, 119°, 140°; 125°, 127°, 108°; 133°, 109°, 119°; 129°, 99° and 132° ± 2°) depart from the angular argument (120°) of a 3‐fold symmetry rotation indicating that, in the close neighbourhood of the QN, the studied arrangement of crystal defects is structurally unstable. Such an instability is associated with an observed mismatch in orientation (by angles of 20°, 15°, 33° and 30° ± 2°) between the TJs and some <111> zone axis matrix lattice crystallographic directions ([], [11], [11] and [11]), respectively). Local variations in anionic composition, existing within the solid solution matrix, are discussed to be responsible for this mismatching and, therefore, for the observed structural instability. 相似文献
996.
Cremona M Mauricio MH Scavarda Do Carmo LC Prioli R Nunes VB Zanette SI Caride AO Albuquerque MP 《Journal of microscopy》2000,197(3):260-267
The influence of the deposition temperature on the grain size of polycrystalline lithium fluoride (LiF) thin films is studied using a mathematical morphology method. On atomic force microscopy images of the LiF surface, the grain sizes and shapes are determined by applying the watershed technique, together with a shape factor algorithm. Also, the domain size of the film structure, determined by an X-ray diffraction data analysis, is compared and correlated with the mean grain size as a function of the deposition temperature. In both cases a linear increase with temperature and a very good agreement among the two structural parameters (grain and domain size) was found. 相似文献
997.
998.
奥氏体锰钢耐磨性的几点评述 总被引:1,自引:0,他引:1
本文通过对几种在相同载荷条件下 ,不同的热处理情况下的磨损以及不同载荷下相同热处理的磨损情况 ,从实验的数据中分析常规高锰和合金高锰钢形变硬化的差异 ,以及这两种锰钢在磨粒磨损时表面产生两种不同现象的分析。比较出4 5 #淬火钢、高速钢、合金高锰钢 ,常规高锰钢耐磨性的不同 相似文献
999.
A stochastic model for simulating the microstructure formation of Mg alloy AZ91 during solidification was developed based on the finite element method(FEM) for macroscopic model of heat transfer calculation and a modified Cellular Automaton (mCA) for microscopic modeling of nucleation, growth of crystal. In this model, the effect of solute redistribution, interface curvature and preferred orientation was considered. A numerical simulation was developed with C++ program language. The computation was carded out to understand the effect of varying processing parameters, such as nucleation parameters and heat transfer coefficient, on the microstructure formation of AZ91. The result of simulation was displayed on screen. 相似文献
1000.